Synthesis of Nanocrystalline Titania via Microwave-Assisted Homogeneous Hydrolysis Under Hydrothermal Conditions

ISSN: 2213-3364 (Online)
ISSN: 2213-3356 (Print)


Volume 1, 2 Issues, 2014






Current Microwave Chemistry

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Editor-in-Chief:
Bimal K. Banik
Department of Chemistry
College of Science & Mathematics
The University of Texas-Pan American
1201 West University Drive
Edinburg, Texas
USA


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Synthesis of Nanocrystalline Titania via Microwave-Assisted Homogeneous Hydrolysis Under Hydrothermal Conditions

Author(s): Moskalenko E.A., Sadovnikov A.A., Baranchikov A.E., Goldt A.E., Kozik V.V. and Ivanov V.K.

Affiliation: Kurnakov Institute of General and Inorganic Chemistry, Leninsky, 31, Moscow, 119991, Russia.

Abstract

In this paper, we report on a new procedure for nanocrystalline titania synthesis using microwave-assisted homogeneous hydrolysis under hydrothermal conditions. We show that this synthetic procedure promotes formation of low-aggregated TiO2 powders with very high specific surface area (up to 240 m2/g) and small particle size (5–7 nm), and that it hinders SO42– ions’ sorption on the surface of nanoparticles.

Keywords: Titania, microwave-hydrothermal synthesis, hexamethylenetetramine, homogeneous hydrolysis, nanocrystalline materials

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Article Details

Volume: 1
First Page: 1
Last Page: 6
Page Count: 6
DOI: 10.2174/2213335601666140404163607
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